Publications

  1. C. Edge, S. Heartz, A. Lagalante, A. Lewis, J. Sweeney “Risk of imidacloprid to soil invertebrates when applied as basal bark spray for the control of Hemlock Woolly Adelgid.” Canadian Journal of Forest Research, accepted, (2025).
  2. K.A Frederick, J. Lubniewski, L. Quimby, R. MacNamara, I. Berry and A.F. Lagalante “Collaborations with Art Museums: A Course-Based Undergraduate Research Experience for Undergraduate Analytical Chemistry” Analytical and Bioanalytical Chemistry, 431, 231-236 (2025).
  3. L.J. Silverberg, T.K. Mal, A.F. Lagalante, M.A. Olsen, M. Fleming, T. Garcia, A. Gavalis, K. Gonzales, C. Gregory, L. Hackenberg, M. Lawlor, E. Li, E. Louca, S. Mack, K. Perhonich, K. Shaffer, C. Thompson, S. Tran, E. Vidala “T3P-Promoted Synthesis of a Series of Novel 3-Aryl-2-phenyl-2,3,5,6-tetrahydro-4H-1,3-thiazin-4-ones“”” Journal of Heterocyclic Chemistry, (2025).
  4. H.P. Yennawar, T.K. Mal, M.A. Olsen, A.F. Lagalante, E.M. Louca, A.D. Gavalis and L.J. Silverberg “Synthesis and crystal structures of two racemic 2-heteroaryl-3-phenyl-2,3-dihydro-4H-pyrido[3,2-e][1,3]thiazin-4-ones” Acta Crystallographica Section E, 80(7), 1-5 (2024).
  5. S. Dowd, L. Lagalante, J. Rahlfs, C. Sharo, D. Opulente, A. Lagalante and J. Elmer “Sequencing of the Lumbricus terrestris genome reveals degeneracy in its erythrocruorin genes” Biochemie, 219, 130-141 (2024).
  6. J. Perier, A.F. Lagalante, E. McCarty, A. Simmons and D. Riley “Uptake and Retention of Imidacloprid and Cyantraniliprole in Cotton (Gossypium hirsutum) for the Control of Bemisia tabaci (Hemiptera: Aleyrodidae)” Journal of Entomological Science, 58(4), 434 (2023).
  7. R.S. Grady, T. Traustadottir, A.F. Lagalante and A.L. Eggler “Blocking thiols enhances bioavailable sulforaphane quantitation in plasma by LC-MS/MS” Journal of Agricultural and Food Chemistry, 71(34), 12875-12882 (2023).
  8. H.P. Yennawar, T.K. Mal, C.N. Pacheco, A.F. Lagalante, M.A. Olsen, M.W. Russell, G.C. Muench, Q.J. Moyer and L.J. Silverberg “Crystal Structures of the Sulfones of 2,3-Diphenyl-2,3-dihydro-4H-1,3-benzothiazin-4-one and 2,3-Diphenyl-2,3-dihydro-4H-pyrido[3,2-e][1,3]thiazin-4-one” Acta Crystallographica Section E, 79(3), 221-225 (2023).
  9. L.J. Silverberg, T.K. Mal, C.N. Pacheco, H.P. Yennawar, A.F. Lagalante, M.A. Olsen, M.W. Russell, H.F. E.N. Yeagley and E.L. Zeigler “Novel Conversion of 2,3-Diaryl-2,3-dihydro-1,3-thiaza-4-ones to Dimeric Ring-opened Thioacetals“ Results in Chemistry, 6, 101062 (2023).
  10. L.J. Silverberg, T.K. Mal, C.N. Pacheco, M.L. Povelones, M.F. Malfara, A.F. Lagalante, M.A. Olsen, H.P. Yennawar, H.F. Sobhi, K.R. Baney, R.L. Bozeman, C.S. Eroh, M.J. Fleming, T.L. Garcia, C.L. Gregory, J.E. Hahn, A.M. Hatter, L.L. Johns, T.L. Klinger, J.J. Li, A.J. Menig, G.C. Muench, M.E. Ramirez, J.  Reilly, N. Sacco, A. Sheidy, M.M. Stoner, E.N. Thompson and S.F. Yazdani “T3P-Promoted Synthesis of a Series of 2-Aryl-3-phenyl-2,3-dihydro-4H-pyrido[3,2-e][1,3]thiazin-4-ones and Their Activity against the Kinetoplastid Parasite Trypanosoma brucei” Molecules, 26(20), 6099 (2021).
  11. M.F. Malfara, L.J. Silverberg, J. DiMaio, A.F. Lagalante, M.A. Olsen, E. Madison and M.L. Povelones “2,3-Diphenyl-2,3-dihydro-4H-1,3-thiaza-4-one heterocycles inhibit growth and block cytokinesis in kinetoplastid parasites” Molecular Biochemical Parasitology, 245, 111396 (2021).
  12. B.N. Sundberg and A.F. Lagalante, “Characterization of non-ionic surfactants in Winsor & Newton’s water-mixable oil paints” Journal of Cultural Heritage, 48, 54-64, (2021).
  13. L.A. Lagalante, A.J. Lagalante and A.F. Lagalante, “3D printed solid-phase extraction sorbents for removal of volatile organic compounds from water” Journal of Water Process Engineering, 35, 101194 (2020).
  14. B.N. Sundberg and A.F. Lagalante “Coaxial Electrospray Ionization for the Study of Rapid In-Source Chemistry” Journal of The American Society for Mass Spectrometry 29(10), 2023-2029 (2018).
  15. K. Watts and A.F. Lagalante “Method Development for Binding Media Analysis in Painting Cross-Sections by Desorption Electrospray Ionization-Mass Spectrometry (DESI-MS)” Rapid Communications in Mass Spectrometry  32(16), 1324-1330 (2018).
  16. J.A. Tasca, C.R. Smith, E.A. Burzynski, B.N. Sundberg, A.F. Lagalante, T. Livshultz and K.P.C. Minbiole “HPLC-MS detection of pyrrolizidine alkaloids and their N-oxides in herbarium specimens dating back to the 1850s” Applications in Plant Sciences 6(4), e1143 (2018).
  17. K.C. Cannon, A. Alkurdi, H. Himel, I. Kurochka, S. Liu, M. Costa, B. Sundberg and A.F. Lagalante “Selective Synthesis of Ortho-substituted 2-Aryl-3-phenyl-1,3-thiazolidin-4-one Sulfoxides and Sulfones by S-Oxidation with Oxone” International Journal of Chemistry 9(4), 87-97 (2017).
  18. H.J. Eichman, B.J. Eck and A.F. Lagalante “A Comparison of ESI, APCI, and APPI Ionization for the LC-MS/MS Analysis of Bisphenols. Application to Bisphenols in Thermal Paper Receipts and U.S. Currency Notes” Rapid Communications in Mass Spectrometry 31(20), 1773-1778 (2017).
  19. K.C. Cannon, M. Costa, M. Pepper, J. Toovy, R.S. Selinsky and A.F. Lagalante “Selective Synthesis of 3-Aryl-2-phenyl-1,3-thiazolidin-4-one Sulfoxides and Sulfones by S-Oxidation with Oxone” International Journal of Chemistry 9(4), 1-11 (2017).
  20. A.F. Lagalante and R.C. Wolbers, “Particle-Based Silicone Cleaning Emulsions. Studies in Model Paint Systems for the Cleaning of Water Sensitive Artworks” in Gels in the Conservation of Art, Eds. Lora Angelova, Bronwyn Ormsby, Joyce Townsend and Richard Wolbers, Archetype Publications: London, 193-199 (2017) .
  21. R. Turcotte, A. Lagalante, J. Jones, T. Elliot, A. Billings and Y. Park “Spatial and Temporal Distribution of Imidacloprid within the Crown of Eastern Hemlock” Journal of Insect Science 17(1), 1–7 (2017).
  22. A.F. Lagalante and R.C. Wolbers, “The Cleaning of Acrylic Paintings. New Particle-Based Water-in-Oil Emulsifiers” in Dall’olio all’acrilico, dall’impressionismo all’arte contemporanea. Studi, ricerche, indagini scientifiche ed interventi conservativ, Proceedings of VII Congresso Internazionale Colore e Conservazione (CESMAR7), il prato Publishing, Milan (2016) p. 163-176.
  23. I. Ziraldo, K. Watts, A. Luk, A.F. Lagalante and R.C. Wolbers “The influence of temperature and humidity on swelling and surfactant migration in acrylic emulsion paint films” Studies in Conservation 61(4), 209-221 (2016).
  24. E.P. Benton, J.F. Grant, R.S. Cowles,  R.J. Webster, R.J. Nichols, A.F. Lagalante and  C.I. Coots “Assessing relationships between tree diameter and long-term persistence of imidacloprid and olefin to optimize imidacloprid treatments on eastern hemlock” Forest Ecology and Management 370, 12-23 (2016).
  25. E.P. Benton, J.F. Grant, R.J. Webster, R.S. Cowles, A.F. Lagalante, A.M Saxton, R.J. Nichols and  C.I. Coots “Hemlock Woolly Adelgid (Hemiptera: Adelgidae) Abundance and Hemlock Canopy Health Numerous Years After Imidacloprid Basal Drench Treatments: Implications for Management Programs” Journal of Economic Entomology 109(5), 2125-2136 (2016).
  26. C. Mannikarottu, J. Tierney, K. Cannon, L. Mascavage and A. Lagalante “A Study of 13C Chemical Shifts for a Series of 2-(4-methoxyphenyl)-substituted-3-phenyl-1,3-thiazolidin-4-ones” International Journal of Chemistry 8(2), 43-50 (2016).
  27. L.J. Silverberg, C. Pacheco, A. Lagalante, J. Tierney, J.T. Bachert, J.A. Bayliff, R.V. Bendinsky, A.S. Cali, L. Chen, A.D. Cooper, M.J. Minehan, C.R. Mroz, D.J. Noble, A.K. Weisbeck, Y. Xie and Z. Yanga “Synthesis and spectroscopic properties of a series of novel 2-aryl-3-phenyl-2,3-dihydro-4H-1,3-benzothiazin-4-ones” ARKIVOK 6, 122-143 (2016).
  28. M. Rotella, A. Briegel, J. Hull, A. Lagalante and R. Giuliano “Synthesis and antibacterial activity of antibiotic-functionalized graphite nanofibers” Journal of Nanomaterials 2015, 1-10 (2015).
  29. L.J. Silverberg, C.N. Pacheco, A. Lagalante, K.C. Cannon, J.T. Bachert, Y. Xie, L. Baker and J.A. Bayliff “Synthesis and Spectroscopic Properties of 2,3-Diphenyl-1,3-thiaza-4-one Heterocycles” International Journal of Chemistry 7(2), 150-162 (2015).
  30. K. Cannon, D. Gandla, S. Lauro, L. Mascavage, L. Silverberg, J. Tierney and A. Lagalante “Selective Synthesis of Ortho-substituted 3-Cyclohexyl-2-phenyl-1,3-thiazolidin-4-one Sulfoxides and Sulfones by S-Oxidation with Oxone” International Journal of Chemistry 7(2), 73-84 (2015).
  31. E.P. Benton, J.F. Grant, R.J. Webster, R.J. Nichols, R.S. Cowles,  A.F. Lagalante and  C.I. Coots “Assessment of Imidacloprid and Its Metabolites in Foliage of Eastern Hemlock Multiple Years Following Treatment for Hemlock Woolly Adelgid, Adelges tsugae, in Forested Conditions” Journal of Economic Entomology 108(6), 2672-2682 (2015).
  32. L.J. Silverberg, K.A. Kistler, K.A. Brobst, H. Yennawar, A.F. Lagalante, G. He, K. Ali, A. Blatt, S.B. Foster, D.B. Grossman, S. Hegel, M.J. Minehan, D. M. Valinsky and J.G. Yeasted “Reactions of the halonium ions of carenes and pinenes: an experimental and theoretical study” European Journal of Chemistry 6(4), 430-443 (2015).
  33. C.E. Dillon, A.F. Lagalante and R.C. Wolbers “Aqueous cleaning of acrylic emulsion paint films. The effect of solution pH, conductivity and ionic strength on film swelling and surfactant removal” Studies in Conservation 57(1), 52-62 (2014).
  34. B.M. Eisenback, S.M. Salom, L.T. Kok and A.F. Lagalante “Impacts of Trunk and Soil Injections of Low Rates of Imidacloprid on Hemlock Woolly Adelgid (Hemiptera: Adelgidae) and Eastern Hemlock (Pinales: Pinaceae) Health” Journal of Economic Entomology 107(1), 250-258 (2014).
  35. T.P. Umile, P.J. McLaughlin, K.R. Johnson, S. Honarvar; A.L. Blackman, E.A. Burnynski, R.W. Davis, T.L. Teotonio, G.W. Hearn, C.A. Hughey, A.F. Lagalante, and K.P.C. Minbiole “Nonlethal Amphibian Skin Swabbing of Cutaneous Natural Products for HPLC Fingerprinting” Analytical Methods 6, 3277-3284 (2014).
  36. D. McGarity, J. Tierney and A. Lagalante “An Anomalous Hammett Correlation for a Series of Substituted 3-Benzyl-2-phenyl-1,3-thiazolidin-4-ones” International Journal of Chemistry 6(4), 1-7 (2014).
  37. R.S. Cowles, A. Lagalante and K. Lombard “Imidacloprid contamination of maple sap following Asian longhorned beetle quarantine treatment” Maple Syrup Digest 26A(3), 22-27 (2014).
  38. R.C. Wolbers, A. Norbutus and A. Lagalante “Cleaning of Acrylic Emulsion Paints: Preliminary Extractive Studies with Two Commercial Paint Systems”, New Insights into the Cleaning of Paintings: Proceedings from the Cleaning 2010 International Conference, Universidad Politécnica de Valencia and Museum Conservation Institute, Eds. Marion F. Mecklenburg, A. Elena Charola, and Robert J. Koestler, Smithsonian Contributions to Museum Conservation: Washington DC, (2013).
  39. L.J. Silverberg, E.R. Bear, K.N. Foose, K.A. Kirkland, R.R. McElvaney, K. Cannon, J. Tierney, S. Lascio, K. Mesfin, D. Mitchell, S. Sharkey, L. So, J. Treichel, M. Waxman, A.F. Lagalante “Verifying the predictability of the 13C chemical shifts for a series of substituted-2-(4-chlorophenyl)-3-phenyl-1,3-thiazolidin-4-ones” International Journal of Chemistry 5(4), 120-127 (2013).
  40. K. Cannon, L. Mascavage, J. Tierney, K. Kistler, H. Yennawar, and A. Lagalante “An Experimental and Theoretical Conformational Study of a Series of Substituted 3-cyclohexyl-2-phenyl-1,3-thiazolidin-4-ones” International Journal of Chemistry 5(3), 1-11 (2013).
  41. C.A. Kelly, A.J. Norbutus, A.F. Lagalante and V.K. Iyengar “Male courtship pheromones are indicators of genetic quality in an arctiid moth (Utetheisa ornatrix)” Behavioral Ecology 23(5), 1009-1014 (2012).
  42. A.F. Lagalante, C.S. Shedden, and P.W. Greenbacker “Levels of Polybrominated Diphenyl Ethers (PBDEs) in Dust from Personal Automobiles in Conjunction with Studies on the Photochemical Degradation of Decabromodiphenyl Ether (BDE-209)” Environment International 37(5), 899-906 (2011).
  43. A.M. Grannas and A.F. Lagalante “So These Numbers Really Mean Something? A Role Playing Scenario-Based Approach to the Undergraduate Instrumental Analysis Laboratory” Journal of Chemical Education 87(4), 416-418 (2010).
  44. F.C. Calvosa and A.F. Lagalante “Supercritical Fluid Extraction of Polybrominated Diphenyl Ether (PBDE) Levels from House Dust with 1,1,1,2-Tetrafluoroethane (R134a)” Talanta 80(3), 1116-1120 (2010).
  45. M. Eisenback, S.M. Salom, L.T. Kok and A.F. Lagalante “Lethal and sublethal effects of imidacloprid on hemlock woolly adelgid (Adelges tsugae, Hemiptera: Adelgidae) and two introduced predator species in the laboratory” Journal of Economic Entomology 103(4), 1222-1234 (2010).
  46. A.F. Lagalante T.D. Oswald, and F.C. Calvosa “Polybrominated Diphenyl Ether (PBDE) Levels in Dust from Previously Owned Automobiles at United States Dealerships” Environment International 35(3), 539-544 (2009).
  47. A.F. Lagalante and T.D. Oswald “Analysis of Polybrominated Diphenyl Ethers (PBDEs) by Liquid Chromatography with Negative-Ion Atmospheric Pressure Photoionization Tandem Mass Spectrometry (LC/NI-APPI/MS/MS): Application to House Dust” Analytical and Bioanalytical Chemistry 391(6), 2249-2256 (2008).
  48. J. Tierney, V. Koyfman, K. Cannon, L.M. Mascavage, and A.F. Lagalante “A Second Study – Predicting the 13C Chemical Shifts For a Series of Substituted-3-(4-methoxyphenyl)-2-phenyl-1,3-thiazolidin-4-ones” Heterocyclic Communications 14(6), 452-460 (2008).
  49. T. Rowhani and A.F. Lagalante “A Colorimetric Assay for the Determination of Polyhexamethlene Biguanide in Pool and Spa Water using Nickel-Nioxime” Talanta 71(2), 964-970 (2007).
  50. A.F. Lagalante and P.W. Greenbacker “Flow injection analysis of imidacloprid in natural waters and agricultural matrixes by photochemical dissociation, chemical reduction, and nitric oxide chemiluminescence detection” Analytica Chimica Acta 590, 151-158 (2007).
  51. J. Tierney, N. Colasante, J. Eagles, S. Kelly, G. Lehmike, O. Lucas, C. Mannikarottu, O. Mehmood, M.D. Nguyen, V. Raj, J. Tsai, V. Koyfman, L.M. Mascavage, and A.F. Lagalante “Substituent Effects Using 13C Chemical Shifts for a Series of Substituted 2-Phenyl-3-pyridyl-1,3-thiazolidin-4-ones with a Comparison to Similarly Substituted 1,3-thiazolidin-4-ones” Heterocyclic Communications 13(6), 335-342 (2007).
  52. A.F. Lagalante, M.E. Montgomery, F. Calvosa and M. Mirzabeigi “Characterization of Terpenoid Volatiles from Cultivars of Eastern Hemlock (Tsuga canadensis)” Journal of Agricultural and Food Chemistry 55(26), 10850-10856 (2007).
  53. A.F. Lagalante, N. Lewis, M.E. Montgomery and K.S. Shields “Temporal and Spatial Variation of Terpenoids in Eastern Hemlock (Tsuga canadensis) in Relation to Feeding by Adelges tsugae” Journal of Chemical Ecology 32(11), 2389-2403 (2006).
  54. A.F. Lagalante and M.A. Felter “Silylation of acrylamide for analysis by solid-phase microextraction/gas chromatography/ion-trap mass spectrometry” Journal of Agricultural and Food Chemistry 52(12), 3744-3748 (2004).
  55. A.F. Lagalante and M.E. Montgomery “Analysis of Terpenoids from Tsuga Species by Solid-Phase Microextraction/Gas Chromatography/Ion-Trap Mass Spectrometry” Journal of Agricultural and Food Chemistry 51(8), 2115-2120 (2003).
  56. B.F. Graham, J.M. Harrowfield, R.D. Trengrove, A.F. Lagalante and T.J. Bruno “Evidence of a Host:Guest Complex Formation Between Carbon Dioxide and the p-t-Butylcalixarenes” Journal of Inclusion Phenomena 43(3-4), 179-182 (2002).
  57. A.F. Lagalante, A. Abdulagatov, and T.J. Bruno “Kamlet-Taft Thermosolvatochromic Parameters of Hydrofluoroethers and Hydrofluoroether Azeotropic Mixtures” Journal of Chemical and Engineering Data 47(1), 47-51 (2002).
  58. W.C. Andersen, R.E. Sievers, A.F. Lagalante, and T.J. Bruno “Solubilities of Cerium(IV), Terbium(III), and Iron(III) ß-Diketonates in Supercritical Carbon Dioxide” Journal of Chemical and Engineering Data 46(5), 1045-1049 (2001).
  59. A.F. Lagalante, M. Spadi and T.J. Bruno “Kamlet-Taft Solvatochromic Parameters of Eight Alkanolamines” Journal of Chemical and Engineering Data 45(2), 382-385 (2000).
  60. A.F. Lagalante, A.M. Clarke and T.J. Bruno “Modeling the Water-R143a Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 103(34), 7319-7323 (1999).
  61. A.F. Lagalante “Atomic Absorption Spectroscopy: A Tutorial Review” Applied Spectroscopy Reviews 34(3), 173-190 (1999).
  62. A.F. Lagalante “Atomic Emission Spectroscopy: A Tutorial Review” Applied Spectroscopy Reviews 34(3), 191-207 (1999).
  63. A.F. Lagalante, R.L. Hall and T.J. Bruno “Kamlet-Taft Solvatochromic Parameters of the Sub- and Supercritical Fluorinated Ethane Solvents” Journal of Physical Chemistry, B 102(34), 6601-6604 (1998).
  64. B.F. Graham, J.M. Harrowfield, R.D. Trengrove, A.F. Lagalante and T.J. Bruno “Solubility of p-t-Butylcalix[n]arenes (n=4,6,8) in Supercritical Carbon Dioxide: A Comparison of Static and Dynamic Measurement Techniques” Fluid Phase Equilibria 151(2), 829-838 (1998).
  65. A.F. Lagalante, A.M. Clarke and T.J. Bruno “Modeling the Water-R134a Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 102(44), 8889-8892 (1998).
  66. A.F. Lagalante, C. Wood, A.M. Clarke and T.J. Bruno “The Kamlet-Taft Solvatochromic Parameters for 25 Glycol Ether Solvents and Glycol Ether Aqueous Solutions” Journal of Solution Chemistry 27(10), 887-900 (1998).
  67. A.F. Lagalante and T.J. Bruno “Modeling the Water-Supercritical CO2 Partition Coefficients of Organic Solutes using a Linear Solvation Energy Relationship” Journal of Physical Chemistry, B 102(6), 907-909 (1998).
  68. A.F. Lagalante, R.J. Jacobson and T.J. Bruno “UV/Vis Spectroscopic Evaluation of 4-Nitropyridine N-Oxide as a Solvatochromic Indicator for the Hydrogen-Bond Donor Ability of Solvents“ Journal of Organic Chemistry 61(18), 6404-6406 (1996).
  69. A.F. Lagalante, B.N. Hansen, T.J. Bruno and R.E. Sievers “Solubility of Copper(II) and Chromium(III) ß-Diketonates in Supercritical Carbon Dioxide” Inorganic Chemistry 34(23), 5781-5785 (1995).
  70. B.N. Hansen, A.F. Lagalante, T.J. Bruno and R.E. Sievers “High-Pressure Cell for Solubility Measurements in Supercritical Fluids” Reviews of Scientific Instrumentation 65(6), 2112-2114 (1994).
  71. B.M. Hybertson, K.S. Rutledge, C.J. Beehler, J.E. Repine, A.F. Lagalante and R.E. Sievers “Pulmonary Drug Delivery of Fine Aerosol Particles from Supercritical Fluids” Journal of Aerosol Medicine 6(4), 275-283 (1993).
  72. R.E. Sievers, S.B. Turnipseed, L. Huang and A.F. Lagalante “Volatile Barium ß-Diketonates for Use as MOCVD Precursors” Coordination Chemistry Reviews 128(1-2), 285-291 (1993).